Golden experiment reveals the invisible forces holding the universe together

Scientists in Sweden have developed a simple method to make the universe’s normally invisible binding forces visible by using gold flakes, salt water and light. The Chalmers University of Technology team created a platform that displays these tiny forces—often described as “nature’s invisible glue,” responsible for effects like dust sticking to surfaces or lizards climbing walls—as shifting colors. The technique offers a faster, more accessible way to study how matter organizes itself at the smallest scales.

Inside the lab, doctoral student Michaela Hošková holds up a small glass container filled with millions of micrometer-sized gold flakes suspended in a salt solution. Using a pipette, she places a droplet of the mixture onto a gold-coated glass plate positioned under an optical microscope. The flakes are immediately drawn toward the surface but stop just short of fully attaching, leaving nanometer-sized gaps between the flakes and the gold substrate.

These tiny liquid-filled gaps act like miniature light chambers. Light reflects back and forth inside them, producing visible colors. When the setup is illuminated with a halogen lamp and the reflected light is analyzed with a spectrometer, the different wavelengths become clear. On the connected monitor, flakes shimmer and shift in colors such as red and green against a golden yellow background.

“What we are seeing is how fundamental forces in nature interact with each other. Through these tiny cavities, we can now measure and study the forces we call ‘nature’s glue’ – what binds objects together at the smallest scales. We don’t need to intervene in what is happening, we just observe the natural movements of the flakes,” says Michaela Hošková, a doctoral student at the Department of Physics at Chalmers University of Technology.

By examining the light captured in the cavities, the team can analyze the balance between two competing forces – one that pulls the flakes together and one that keeps them apart. The attractive force, known as the Casimir effect, causes the gold flakes to move toward each other and toward the surface. The opposing electrostatic force develops in the salt solution and prevents the flakes from fully sticking. When these forces reach equilibrium, a process called self-assembly occurs, forming the cavities that make the measurements possible.

“Forces at the nanoscale affect how different materials or structures are assembled, but we still do not fully understand all the principles that govern this complex self-assembly. If we fully understood them, we could learn to control self-assembly at the nanoscale. At the same time, we can gain insights into how the same principles govern nature on much larger scales, even how galaxies form,” says Michaela Hošková.

The new platform builds on several years of research in Professor Timur Shegai’s group at the Department of Physics. Four years ago, the team showed that a pair of gold flakes could form a self assembled resonator. They have now expanded that discovery into a broader method for investigating fundamental forces.

In this system, the gold flakes function as tiny floating sensors. According to the researchers, the approach could be valuable across physics, chemistry, and materials science.

“The method allows us to study the charge of individual particles and the forces acting between them. Other methods for studying these forces often require sophisticated instruments which cannot provide information down to the particle level,” says research leader Timur Shegai.

The platform may also help scientists better understand how particles behave in liquids, including whether they remain stable or tend to clump together. That knowledge could improve how medicines move through the body, support the design of more effective biosensors, and contribute to better water filtration systems. It is also relevant for everyday products such as cosmetics, where preventing unwanted clumping is essential.

“The fact that the platform allows us to study fundamental forces and material properties shows its potential as a truly promising research platform,” says Timur Shegai.

In the laboratory, Hošková opens a small box containing a finished version of the device. Using tweezers, she places it into the microscope. Two thin glass plates enclose everything needed to examine nature’s invisible glue.

“What I find most exciting is that the measurement itself is so beautiful and easy. The method is simple and fast, based only on the movement of gold flakes and the interaction between light and matter,” says Michaela Hošková, zooming in on a gold flake whose colors immediately reveal the forces at work.

Gold flakes about 10 micrometers in size are placed in a salt solution, meaning water that contains free ions. When a droplet is added to a gold-coated glass surface, the flakes are drawn toward it, and nanometer-sized cavities (100-200 nanometers) form. This self assembly results from the balance between two forces: the Casimir force, a measurable quantum effect that pulls objects together, and the electrostatic force that arises between charged surfaces in a salt solution.

A halogen lamp shines light into the cavities, where it becomes trapped and reflected. An optical microscope and spectrometer then separate the light into its component wavelengths so the colors can be identified. By adjusting the salt concentration and observing how the flakes shift relative to the surface, researchers can measure the underlying forces. To prevent evaporation, the droplet containing the gold flakes is sealed and covered with a second glass plate.

The platform was developed at Chalmers’ Nanofabrication Laboratory, Myfab Chalmers, and at the Chalmers Materials Analysis Laboratory (CMAL).

For more information: PNAS

Image: Researchers at Chalmers University of Technology, Sweden, have discovered a quick and easy way to study the hidden forces that bind the smallest objects in the universe together. Using gold, salt water, and light, they have created a platform on which the forces can be seen through colors. Two thin glass plates hold everything needed to study nature’s invisible glue. Credit: Chalmers University of Technology | Mia Halleröd Palmgren

Scientists develop inexpensive, high-quality lenses for super-resolution microscopy

Researchers at the University of Strathclyde in Glasgow, U.K., have shown that consumer-grade 3D printers and low-cost materials can be used to produce multi-element optical components that enable super-resolution imaging, with each lens costing less than $1 to produce. The new fabrication approach could broaden access to fully customizable optical parts and enable completely new types of imaging tools.

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Research team shows nanoparticles adhere to quantum mechanics

Researchers at the University of Vienna have demonstrated quantum interference in sodium nanoparticles containing more than 7,000 atoms—and produced clusters of nearly 10,000—showing that even large metallic particles can exhibit quantum behavior. Lead author Sebastian Pedalino said the results challenge the assumption that such objects must behave classically, confirming that quantum mechanics remains valid at this scale without the need for alternative models. 

The team, led by Markus Arndt and Stefan Gerlich, achieved the breakthrough using sodium clusters exceeding 170,000 atomic mass units, larger than most proteins, marking a significant advance toward the long-sought goal of sustaining quantum superposition in increasingly complex systems.

The test was conducted using the multi-scale cluster interference experiment (MUSCLE). 

To observe interference, the team had to minimize environmental disturbances that would destroy coherence. They produced the sodium clusters under cryogenic conditions (77 K, the temperature of liquid nitrogen) to reduce thermal decoherence, and ran the interferometer in ultra-high vacuum (about 9 × 10⁻⁹ mbar, roughly 10⁻¹¹ of atmospheric pressure) to limit collisions with gas molecules.

The scientists produced sodium clusters containing roughly 5,000 to 10,000 atoms and sent them through a three-grating interferometer made from standing ultraviolet laser light. The first grating spatially confined the particles to build up coherence, and the second grating acted as a beam splitter for the clusters’ matter wave. Scanning the third grating revealed an interference fringe pattern, and the team showed the fringe visibility followed the quantum prediction rather than a classical shadow-pattern model

The study achieved a macroscopicity value of 15.5. This metric quantifies how strictly an experiment tests the limits of quantum theory. This study has a value 10 times higher than any previous experiment. 

This new level of sensitivity presents new opportunities for nanotechnology and materials science, opening new doors for measuring properties of nanoparticles and investigating the transition of matter from individual atoms to bulk metallic solids. 

For more information: University of Vienna

Image: MUSCLE at the University of Vienna, where quantum interference of massive nanoparticles was detected. To isolate vibrations, the experiment is mounted on a table weighing several tons that floats on an air cushion. Credit: S. Pedalino / Uni Wien

New nanoprobing platform for high voltage applications

Imina Technologies SA, Switzerland, released a new Nanoprobing High-Voltage Platform designed to safely apply voltages up to 1 kV through both nanoprobing tips and the backside of the sample, addressing the growing need for reliable electrical characterization of wide-bandgap and high-power semiconductor devices such as SiC- and GaN-based MOSFETs, IGBTs, and other devices.

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Ferroelectric materials boost data storage potential

Researchers at Oak Ridge National Laboratory, Oak Ridge, Tenn., modified a commercial atomic force microscope with artificial intelligence to assemble and detect patterns in bismuth ferrite and analyze defects at the materials’ surface, advancing the understanding of these materials and enabling innovative data storage and computation methods.

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Intertek Caleb Brett opens new laboratory in Naples, Italy

Intertek, UK, a leading Total Quality Assurance provider to industries worldwide, announced the opening of a new Intertek Caleb Brett laboratory in Naples, Italy, strengthening its presence in this important region and addressing a growing demand for reliable, high-quality testing services in crude oil, refined fuels, and emerging biofuels.

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Observing gold’s atomic structure change at extreme pressures

Researchers at Lawrence Livermore National Laboratory (LLNL) and their collaborators conducted experiments with gold to learn more about the unexpected structures and properties it would adopt under high pressure. The results, which show gold switching structure at 10 million times the Earth’s atmospheric pressure, are essential for planetary modeling and fusion science.

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Diamond exhibits surprising nanoscopic heat traps

New research shows that diamond—although known for being the best natural heat conductor on Earth—at the atomic scale it can briefly trap heat in unexpected ways. The findings could influence how scientists design diamond-based quantum technologies, including ultra-precise sensors and future quantum computers.

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High-precision analysis of 2D materials microstructures achieved using electron microscopy and machine learning

A research team led by National Institute for Materials Science, Japan, has, for the first time, produced nanoscale images of two key features in an ultra-thin material: twist domains (areas where one atomic layer is slightly rotated relative to another) and polarities (differences in atomic orientation) by combining scanning transmission electron microscopy with artificial intelligence.

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Building a sustainable metals infrastructure: NIST report highlights key strategies

NIST has released a report outlining strategies to build a more efficient, sustainable, and resilient U.S. metals processing infrastructure, emphasizing the need for improved standards for recycled content and stronger supply chains for critical materials. Covering the full lifecycle—from mining and alloy design to manufacturing, reuse, and recycling—the report highlights that addressing these challenges is essential for innovation, industrial competitiveness, and national security. The findings stem from a NIST workshop held in July 2024.

“The workshop brought together a diverse group of experts from industry, academia and the policy world to take on some of the biggest challenges in the metals processing space,” said NIST materials research engineer Andrew Iams, a co-author on the report. “Meeting these challenges requires a new approach in how to source, process, use and recycle metals.”

The report covers various topics related to metals manufacturing, from new technologies for extracting and processing bulk materials, like aluminum and steel, to developing new modeling and data tools to design advanced alloys.

The report highlights the importance of critical materials, including minerals containing lithium and cobalt that are key manufacturing elements for smartphones, batteries, semiconductors and medical devices, as well as superalloys used in military hardware and jet engines.

These materials can be challenging to obtain due to limited availability and the risk of supply chain disruptions. Industries can address these issues by diversifying their supply chains with new sources, identifying substitute materials, and improving recycling methods to enable greater recirculation of existing materials.

The report also highlights the need to improve standards for metals reuse and recycling. Better standards can make the separation of metals for recycling more efficient, reducing industry costs. New certification programs can help ensure that products made with recycled content meet performance standards, which could expand the market for recycled materials.

The report highlights five strategies that would help the industry tackle these and other challenges:

  • Advance measurement science for sustainable metals manufacturing, including new separation techniques for recycling.
  • Develop the technical basis to support standards development, including the data needed to create or improve performance-based standards for highly recycled metals, such as aluminum and steel.
  • Enhance data and modeling tools for addressing supply risks and designing products for improved recyclability.
  • Promote workforce development and education by establishing training programs and creating partnerships between universities, labs and industry.
  • Convene stakeholders to establish collaborations that foster knowledge-sharing and innovation.

The NIST workshop brought together manufacturers, technology companies, researchers and other experts from all stages of the metals processing chain. NIST has a long history of convening stakeholders across industrial sectors to solve shared problems through better technology and standards.

“We are always seeking ways to help industrial partners solve tough engineering or scientific problems,” Iams said. “Part of NIST’s mission is to help keep U.S. industry competitive. We can do that by identifying promising technologies and helping to move them out of the lab so they can be implemented on an industrial scale.”

For more information: Material Challenges in Developing a Sustainable Metal Processing Infrastructure – Workshop Report

Lehigh’s Blacksmithing Club to open its first dedicated lab

Lehigh University’s Blacksmithing Club is set to move into its first dedicated lab space in Whitaker Laboratory, marking a major step for its growing community of student metalworkers. The club, supported by professor Laura Moyer and partnerships with Historic Bethlehem Museums & Sites and Lehigh Heavy Forge, offers hands-on experience in both traditional and modern metalworking. Students have also practiced basic techniques at the historic 1750 Smithy, while The Loewy Institute continues to provide education in advanced metal-forming technology.

Moyer said the team had discussed building a lab for years but wasn’t sure how to achieve it financially or where it would be located. 

With student interest rising, Moyer said the idea for the blacksmithing club started to solidify two years ago when a student — now club president Josh Swavely, ‘26 — mentioned his passion for blacksmithing in one of Misiolek’s classes.

Under the guidance of Moyer and Misiolek, the group helped launch a one-credit blacksmithing elective offered each spring. Moyer said this course, now in its second year, is open to students of all majors, as is the club. 

Moyer also said they are hoping to grow the one-credit course that is currently offered for half a semester into a full-semester three-credit elective for students. 

“Within the course we are developing, the idea is to balance time between the laboratory and the lecture hall, between practice and theory,” Misiolek said. “It will be much more of an opportunity to design your own products, analyze the proposed processes, and learn while you are going through the process.”

Moyer said the new laboratory will allow students to complete every stage of the design cycle in one place — from heating and shaping metal at the forge to examining the microstructure of their finished work.

She said students will also be able to fabricate hooks, blades and small hardware entirely on campus supported by new ventilation hoods, anvils and space for larger tools.

Misiolek said the club’s growth has been driven by access to working forges across Bethlehem. Through its partnership with Historic Bethlehem Museums & Sites, students learn centuries-old techniques at the 1750 Smithy.

He also said their work with the Lehigh Heavy Forge in Bethlehem allows students to witness a modern industrial facility that provides advanced forgings to clients.

“We are connecting the historical aspects of forging technology with hands-on experience and current industrial practices,” Misiolek said. 

He also said beyond traditional forging skills, the new lab will support lessons on heat treatments, controlled cooling and other methods that help students compare how different variables affect the strength and performance of their designs.

Nick Rockwell, a researcher at the Loewy Institute, said community partnerships have been essential in turning the club’s ideas into practice. 

“With all the support we’ve received, it’s really helped us connect with Historic Bethlehem,” he said. 

He also said Mike Rex, the shop and laboratory operations supervisor, has been instrumental in building facilities for the lab and giving advice on how to best use the space.

The club also gives students opportunities beyond the classroom. Members have participated in the Forging Industry Educational and Research Foundation’s annual competition and secured funding from the nonprofit organization to support their work.

“We pride ourselves in our hands-on approach,” Moyer said. “There are a lot of materials science and engineering departments across the country, but many don’t allow undergraduate students into labs or use highly specialized equipment.”

For more information: Lehigh University

Image: Josh Swavely, ’26, is pictured forging a point in the soon to be blacksmithing lab. Swavely is the president of the Lehigh Blacksmithing Club. (Max Randall/B&W Staff)

Using ultrabright X-rays to test materials for ultrafast aircraft

Designing hypersonic aircraft that travel at five to seven times the speed of sound is a major challenge because their materials must be lightweight yet capable of withstanding extreme heat and pressure. To address this, researchers at Embry-Riddle Aeronautical University, in collaboration with the U.S. Department of Energy’s Argonne National Laboratory, are developing a device that simulates the intense thermal and mechanical stresses of hypersonic flight. Paired with the ultrabright X-rays of Argonne’s Advanced Photon Source, this system will allow scientists to observe real-time changes in these materials under flight-like conditions.

“Recreating the environment of hypersonic flight can be complicated,” said Seetha Raghavan, professor of aerospace engineering and a co-principal investigator on the project. ​“There are so many factors and no perfect way to test them all. High enthalpy wind tunnels that can simulate the wind speed use a lot of energy resources and are limited in access.” (Enthalpy refers to the heat content of a system at constant pressure.)

The research team’s goal is an alternative that replicates hypersonic flight conditions using fewer energy resources and uses APS X-rays to capture detailed data. The APS is in the final stages of an upgrade that increased the brightness of its X-ray beams by up to 500 times. It is now the brightest synchrotron X-ray facility in the world, and according to Raghavan, the enhanced capabilities of the upgraded APS are crucial to this project.

“When you are talking about hypersonics, you’re talking about high speeds and fast changes, and response time is critical,” she said. ​“You can only get that kind of time resolution with enough flux (or brightness of the beam), and the upgraded APS is able to help with that.

“Additionally, the materials we’ll be testing are the thinnest that can be used, and at the upgraded APS you can focus the beam down to a small enough size to capture the data we need,” she said.

Victoria Cooley, an APS beamline scientist who worked with the Embry-Riddle team at beamline 1-ID, touted both the upgraded X-ray beam and the improved experiment station.

“It’s an exciting time for our beamline,” she said. ​“Brighter X-rays allow us to probe deep into materials with a higher-resolution beam and map very thin samples like these. At the same time, we have installed faster, more sensitive detectors to capture chemical or crystallographic changes occurring incredibly quickly. These two pieces come together to make world-changing projects such as this one possible.”

Uncovering materials that can withstand the conditions of hypersonic flight and are not prohibitively expensive to produce is key to unlocking their many applications. Durable hypersonic materials could be used for military and civilian aircraft, as well as cargo delivery vehicles.

The hypersonic materials project is supported by a $1.4 million contract from the U.S. Department of War Joint Hypersonics Transition Office through the University Consortium for Applied Hypersonics. The Embry-Riddle team’s principal investigator is William Engblom, professor of aerospace engineering, and Mark Ricklick, associate professor of aerospace engineering, is a co-principal investigator.

For more information: Embry-Riddle

Image: The Embry-Riddle research team at Beamline 1-ID, with Argonne scientist Victoria Cooley (back row, right). (Image by Mark Lopez/Argonne National Laboratory.)

Mapping the future: AI method to transform alloy properties prediction and design

Researchers at The Grainger College of Engineering have integrated their expertise in metals with advanced machine learning to create detailed spatial maps, enabling faster and more precise autonomous material design. Similar to how fingerprint technology captures intricate ridge and valley patterns for biometric identification, their approach leverages spatial mapping of fine details to revolutionize material engineering.

This evolution of recognition technology is mirrored in the field of materials science, where researchers seek new and efficient ways to fully characterize materials, accelerating the discovery of additional new materials. Much like human fingerprints, the performance of metal mixtures called alloys relies on the intricate spatial arrangement of microstructural features. Traditional methods reduce this complexity into a handful of averaged values, causing each alloy to lose its distinctive “fingerprint.”

 In a recent complement of papers from the lab of Jean-Charles Stinville, assistant professor of materials science and engineering, Illinois Grainger engineers have introduced new machine learning approaches for identifying alloy microstructures and predicting their properties rapidly. The Illinois researchers’ method will provide new avenues for faster and more efficient materials design. 

Microstructures are tiny structural features of metals that influence their strength and behavior. Scientists look to the microstructural properties of metals to assess their functionality. Metals used in propulsion devices like rockets and airplanes have special requirements. 

“We are sending these materials into increasingly extreme environments,” Stinville said. “They are exposed to intense environments; for instance, structural materials for space applications must be resistant to mechanical loading under extremely low or high temperatures. Conventional alloys don’t do as well in these conditions because their mechanical properties tend to degrade under these extreme environments. We want to find new ways to accelerate the identification of alloy chemistries and microstructures that can withstand these harsh conditions.”

The complete details of these microstructures, including small-scale influential variances called heterogeneities, cannot be easily captured by existing methods. Instead, Stinville and his colleagues used deep learning to analyze diffraction patterns, or the way electrons interact with metals. By encoding these interactions through a machine learning method onto a spatial latent representation, the researchers captured the full extent of an alloy’s microstructure and its heterogeneity — an approach Stinville calls Material Spatial Intelligence.

“Traditionally, we have used single descriptors or average values to guide data-based alloy design,” he said. “But spatial information from local measurements over a large field of view allows us to capture microstructure heterogeneity of the alloy. Using such spatial information in a data-based model provides significant improvement in prediction accuracy and enables alloy and microstructure design.” 

The initial model is a machine learning approach that successfully identified microstructures and material heterogeneity in unprecedented detail. In a second paper published in Scripta Materialia, Stinville further progressed the model towards the prediction of mechanical properties using the developed approach of material spatial intelligence. This method accelerates alloy property prediction by orders of magnitude and provides a rapid fundamental understanding of structure properties in metals. 

“I started my career as an experimentalist, where I developed tools that allowed us to collect large fields of view with very high resolution,” he said. “Then I went over to the numerical side to develop machine learning tools to actually use all this spatial information. As a metallurgist, I have an understanding that metals are controlled by local properties and their heterogeneities. My unique material scientist background really helped me in developing these novel models.”

By combining high-resolution digital image correlation with alloy microstructure characterization, Stinville examined tiny regions of metal surfaces and how they deformed at a small scale when loaded. Training a new model to recognize these deformation fingerprints allowed him to reliably predict important properties like strength, fatigue life, and ductility (the ability to extend without breaking). The model significantly decreases the time for testing, lessening the time needed to evaluate new alloys. This acceleration brings the field one step closer to intelligent alloy design.

Stinville envisions a future model that works backwards from a user’s desired properties to suggest a chemical composition and microstructure that best suits the given parameters. By integrating these approaches with his group’s advances in automated characterization, Stinville’s lab is setting the stage for fully autonomous alloy design, marking their next frontier.

But even as exciting advancements loom, Stinville still marvels at his field’s early beginnings. 

“This approach unites our field’s fundamental understanding of metals with new and efficient AI database tools,” he said. “We’re not just taking these new tools and leaving behind what we’ve already learned. We’re integrating the present with the past.” 

Mathieu Calvat, Chris Bean and Dhruv Anjaria significantly contributed to this research.

For more information: NPJ Computational Materials

Image: Electron backscatter diffraction (EBSD) maps of the investigated Inconel 718 alloys. Inverse pole figure (IPF) maps along the X direction (horizontal) are presented for a A wrought and fully recrystallized 718 alloy, and a B additively manufactured as-built 718 alloy

AI-generated nanomaterial images fool experts in new study

Microscopy images are indispensable in nanomaterials science. Yet scientists now fear that generative AI is diluting the significance of these images by polluting the pool with fake, AI-generated photos that are indistinguishable from the real ones. Even seasoned researchers find it increasingly difficult to distinguish between real microscopy images of nanomaterials and those created by AI as shown in a new study.

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Electron microscopy reveals new process for developing exotic metal alloys

Researchers from the Department of Energy’s Lawrence Berkeley National Laboratory (Berkeley Lab) have discovered a new way to produce high-entropy alloys (HEAs), at near-room temperatures. Their technique gives users much more control of the alloy’s crystal structure and overall morphology compared with existing methods, opening the door for a new paradigm of custom-made HEAs.

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