OHIO researchers Faiz Rahman, Savas Kaya receive $550,000 NSF award for next-generation nanolithography

A new U.S. National Science Foundation award will support Dr. Faiz Rahman and Dr. Savas Kaya in developing an advanced electron-beam lithography technique capable of creating features smaller than 5 nanometers. The three-year, $550,000 project runs from Sept. 1, 2026, through Aug. 31, 2029.

Electron-beam lithography is an important tool for fabricating extremely small customized structures, but producing features approaching molecular dimensions remains technically challenging.

The new project seeks to overcome these limits by combining a very fine electron beam with deep-ultraviolet radiation and singlet oxygen, a highly reactive form of oxygen. The electron beam breaks long polymer chains in the resist into smaller fragments, while singlet oxygen helps remove those fragments during patterning. This approach could allow extremely small openings to be produced directly in the resist in a single-step process.

The research aims to demonstrate patterning at the sub-5-nm scale, a capability increasingly important for semiconductor manufacturing and potentially valuable in photonics, bioengineering, nanomaterials and biomedical applications. The resulting nanoscale patterns could also be used as templates for removing or depositing materials and for fabricating photomasks needed for future generations of microelectronic devices.

The work will be conducted at Ohio University’s Russ Research Opportunity Center (RROC) and will strengthen NQPI’s experimental capabilities in nanofabrication and nanoscale science.

According to Rahman, an existing scanning electron microscope will be converted into an electron-beam lithography system for the project. The research will also provide training opportunities for postdoctoral and graduate researchers.

The award highlights the interdisciplinary strengths of NQPI and Ohio University in nanotechnology, advanced manufacturing, materials science and device fabrication, while establishing new capabilities for creating structures at dimensions of only a few nanometers.

For more information: National Science Foundation

Locusts get a sensory assist from nanomaterials

Researchers are exploring how insects could serve as sensing systems in environments that are difficult or dangerous for humans to access. Research from Washington University in St. Louis combines insects’ biological abilities with engineering to potentially detect hazards, map areas and gather information in challenging environments.

“We marry the best biology has to offer with engineering principles to create a superior sensing system,” said Barani Raman, the Dennis & Barbara Kessler Professor in biomedical engineering at the WashU McKelvey School of Engineering.

Raman and his colleague Srikanth Singamaneni, the Lilyan & E. Lisle Hughes Professor in mechanical engineering and materials science, are senior authors of the research.

Both biological and artificial chemical sensing systems have drawbacks, Singamaneni said. A locust’s olfactory system is extremely sensitive and can detect faint odors that guide its behavior. But even with 50,000 olfactory receptor neurons in each antenna, it can’t identify a wide enough range of chemical compounds. Meanwhile, synthetic sensors don’t perform as well as more nimble living creatures, but they can be very accurate at detecting specific compounds. Why not combine the two?

“Both biological and artificial chemical sensing approaches have their strengths and drawbacks,” said Singamaneni, but by combining them, “you can cast a broader net.” Here, they added an ultralight, highly porous nanomaterial coating, known as surface-enhanced Raman scattering (SERS) substrate, to the locusts’ antennae.

SERS is a technique that boosts signals from molecules on or near nanostructure metal surfaces; it’s especially useful for detecting trace chemicals. In this case, researchers used a collagen foam applied to the antennae or wings. The foam augmented the insect’s odor-detecting skills without interfering with its other functions.

Singamaneni’s lab specializes in designing and synthesizing these types of nanomaterials. He has been working with plasmonic nanostructures as long as Raman has been mapping locust sensory circuits. They melded their research, and it paid off. Locusts equipped with the foam outperformed non-SERS locusts as well as synthetic chemical sensors, improving odor-detection performance across all chemicals tested, including the chemical signature for TNT.

In a series of tests, their hybrid systems successfully detected a wider range of smells without affecting the insect’s normal functions.

Raman said a key challenge in chemical sensing is they often don’t know what molecules they’re targeting. The foam attached to the antenna helps identify particular chemical species, he noted. The biology and the chemical sensing parts complement each other.

“It clearly showed the best of the two worlds can be merged,” he said.

For more information: Advanced Materials

Image: A future hybrid system could deploy locusts like this one to detect chemical vapors in search-and-rescue operations, or war zones, quickly identifying particular chemicals based on neural response signatures in the organism and pinpointing their locations before responders enter the scene. The foam on the antenna and wing can enhance an organism’s innate sensory system, collect samples and detect trace chemical signatures. (Photo: Raman lab)

A 0.42-nanometer breakthrough could push transistors beyond silicon

A working transistor requires an extremely thin insulating layer known as the gate dielectric. This layer sits above the semiconductor and helps control the movement of electrons. As transistors shrink, making this insulating layer thinner can improve electrical control. The difficulty is that adding such layers to atomically thin semiconductors can disturb the delicate interface between the materials. That disruption can scatter electrons and erase some of the performance gains engineers are trying to achieve.

For years, researchers have therefore faced a difficult tradeoff. They could strengthen control over the transistor gate, or they could protect the mobility of the charge carriers moving through the device. Achieving both at once has been much harder.

Researchers at National Yang Ming Chiao Tung University (NYCU), Taiwan, working with TSMC Corporate Research, Taiwan, have now demonstrated a new way to address this problem by focusing on the interface itself.

The work, published in Nature Electronics, shows that carefully controlling the atomic boundary between a semiconductor and its insulating layer can allow the dielectric to be made extremely thin while maintaining strong electrical performance. Rather than searching for a completely different semiconductor, the researchers concentrated on the narrow region where the two materials meet, an area only a few atoms thick.

Instead of changing either the semiconductor or the gate dielectric, the NYCU researchers redesigned the interface connecting them.

The team first placed an ultrathin epitaxial aluminum layer directly onto monolayer molybdenum disulfide (MoS2). They then carefully oxidized the aluminum, producing an aluminum oxide layer about 0.42 nanometers thick. After that, they added the high κ hafnium oxide gate dielectric.

Despite being only a fraction of a nanometer thick, the engineered interface performs two important jobs.

First, it creates a smooth and continuous surface that allows the hafnium oxide to grow more uniformly over the MoS2. Second, it works as an atomic buffer that limits unwanted electrical interactions between the dielectric and the semiconductor. This protection helps electrons continue moving efficiently through the transistor channel.

In this design, the interface does more than simply keep two materials apart. It becomes a functional part of the transistor and helps the materials work together more effectively.
Using the new interface design, the researchers fabricated short-channel top-gate transistors from CVD-grown monolayer MoS2. The devices had an equivalent oxide thickness of roughly one nanometer.

Testing showed low leakage current, minimal hysteresis, and maximum transconductance of 0.45 mS μm-1 in transistors with channels measuring about 100 nanometers.

More importantly, the devices demonstrated a combination that has been difficult to achieve in atomically thin transistors: very thin dielectric scaling, strong electrostatic control, and sustained carrier transport.

Because the researchers used CVD-grown monolayer MoS2 rather than mechanically exfoliated flakes, they believe the approach brings the technology closer to materials and processes that could eventually be suitable for wafer-scale manufacturing.

The findings also point to a broader change in the way semiconductor researchers think about transistor design.

For decades, much of the effort to improve transistors has centered on discovering better semiconductor materials or making devices smaller. As transistor components approach atomic dimensions, however, the interfaces separating different materials become increasingly important.

These regions may be only a few atoms thick, yet they can strongly influence how well the materials on either side work together. The new results add to growing evidence that controlling these atomic interfaces could become as important as developing new semiconductor materials themselves.

 

Image – Researchers from NYCU and TSMC show that redefining the atomic boundary between materials can address a major engineering barrier restricting the development of next-generation semiconductor devices. Courtesy of: Springer Nature.

 

For more information:

National Yang Ming Chiao Tung University
https://www.nycu.edu.tw/nycu/en/index

New analog memory may make smart devices even smarter

Researchers at Sandia National Laboratories have developed electro-thermo-chemical random-access memory, a technology that uses localized heating and electrical pulses to store a range of analog values instead of binary ones and zeros, making future electronics more energy efficient.

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Penn State, Kurt J. Lesker Company partner to advance atomic-scale processing

Penn State and Kurt J. Lesker Company have launched a strategic partnership to advance atomic-scale materials processing for semiconductors, advanced packaging, quantum technologies and photonics. Central to the collaboration is the new Kurt J. Lesker Company Atomic Scale Processing Center of Excellence, known as ASPIRE, at Penn State. The center will combine the company’s equipment and process expertise with Penn State’s nanofabrication, materials research and characterization capabilities to support next-generation technology development and workforce training. The partnership was formally launched Sept. 9 with the signing of a memorandum of understanding and a ribbon-cutting ceremony at the Millennium Science

KJLC is a Pennsylvania-based company specializing in vacuum science and equipment used to create and shape extremely thin layers of materials. These thin films are essential components in semiconductors and other advanced technologies.

A central goal of the partnership is to develop and validate atomic-scale processing recipes, or detailed instructions for creating thin films with specific properties. These recipes could ultimately be shared with KJLC customers and academic researchers around the world.

The partnership builds on a research relationship, demonstrating the world’s first ferroelectric aluminum-scandium nitride thin films grown by plasma-enhanced atomic layer deposition. The achievement highlights the role of atomic scale processing in enabling next-generation semiconductor, quantum and advanced electronic technologies, according to KJLC and Penn State leadership.

The most recent collaboration will focus on two highly precise processes: atomic layer deposition, which builds thin films a few atoms at a time, and atomic layer etching, which removes material with similar precision. That level of control is critical because even tiny differences in a material’s thickness or composition can affect how well a device performs.

“Few universities offer the combination of research expertise, characterization capabilities and nanofabrication infrastructure available at Penn State,” said Joshua Robinson, director of Penn State’s Materials Research Institute and professor of materials science and engineering. “Coupling those strengths with Kurt J. Lesker Company’s technologies and process engineers creates a unique environment where new ideas can benefit scientific discovery and advance technology development.”

Under the agreement, KJLC will loan three ultra-high purity atomic scale processing tools to the Nanofabrication Laboratory. One 200-millimeter atomic scale processing system integrates both atomic layer deposition and atomic layer etching, enabling researchers to deposit and etch materials with near-atomic precision. Together, the systems are valued at approximately $4.45 million. KJLC will retain ownership and responsibility for maintaining them. Penn State researchers will have access to the three systems for University research, joint projects with KJLC and work conducted for Penn State’s user community.

“From a business perspective, Penn State was the natural choice because of our long-standing relationship and shared commitment to advancing scientific discovery,” said Kurt Lesker IV, president and CEO of Kurt J. Lesker Company. “Through the Materials Research Institute, Penn State brings world-class researchers, advanced nanofabrication capabilities, and a collaborative environment where industry and academia work side by side to solve important challenges. Together, we are creating a center of excellence that will accelerate innovation, develop future talent, and strengthen leadership in semiconductors, advanced packaging and next generation technologies.”

The partnership will also establish workforce development programming for undergraduate and graduate students and early-career professionals, with potential activities including internships and graduate research support.

“KJLC already has considerable training programs in vacuum technologies and deposition,” Robinson said. “By connecting that industry expertise with the research happening at Penn State, we can create new training opportunities for students and the broader workforce.”

Such training opportunities will include learning from Penn State researchers and KJLC engineers, who will use the loaned equipment to develop and test new materials and processing methods for applications including quantum technologies, micro- and nano- scale sensors and mechanical devices, biomedical coatings, advanced packaging and flexible electronics.

“The future of advanced technology will be built one atomic layer at a time,” Lesker said. “By combining Penn State’s research leadership with Kurt J. Lesker Company’s vacuum and thin film expertise in atomic scale processing, we can accelerate the development of new materials and manufacturing processes that enable breakthroughs in semiconductor packaging, quantum technologies, photonics and advanced electronics. Just as importantly, this partnership helps bridge the gap between scientific discovery and real-world application while preparing the next generation of scientists and engineers who will drive innovation for decades to come.”

Penn State and KJLC researchers will use the systems to develop recipes specifying the materials, temperatures, timing and other conditions needed to consistently create a particular thin film or structure. The partners will develop a growing library of standardized atomic-scale processing recipes that can be shared across the research community and ultimately deployed on KJLC platforms worldwide. KJLC will also provide Penn State access to 38 processes it has already developed, and Penn State researchers will be able to draw on KJLC’s principal scientist and other technical experts while developing new ones.

Once a process is developed and refined through the partnership, KJLC could make it available to customers using its equipment elsewhere, extending work done at Penn State to researchers and companies around the world.

For more information: Communications Materials

Image: Andrew Read, Penn State senior vice president for research, right, and Kurt Lesker IV, president and CEO of Kurt J. Lesker Company, left, do a ceremonial ribbon cutting to launch the partnership between Penn State and Kurt J. Lesker Company to develop new ways to create specialized materials for next-generation technologies. Credit: Jennifer M. McCann / Penn State

Scientists are building a microscope powered by a quantum computer

Researchers at TU Wien, in collaboration with the University of Vienna, JKU Linz and the University of Innsbruck, are developing a quantum computer-assisted electron microscope designed to capture additional quantum information carried by electrons that is typically lost in conventional imaging. The approach could produce clearer images while reducing the number of electrons needed, helping protect delicate samples such as biological materials. A prototype quantum computer electron microscope based on the concept is currently under construction at TU Wien.

For more infromation: University of Vienna

Image: An electron microscope capable of performing quantum computing operations using built-in ion traps. Credit: TU Wien

Rice’s Sanchez exploring a future where fabric itself becomes the robot

Rice University Assistant Professor of Mechanical Engineering Vanessa Sanchez has received the Toyota Programmable System Innovation Fellowship to develop advanced 3D-knitted soft robotic textiles that integrate sensing, movement and mechanical functions directly into fabric. The research aims to create textiles that can adapt to users’ needs, such as enhancing mobility, improving comfort and increasing safety, with the long-term goal of making the textile itself function as a robot.

“We tend to think of fabric as something passive — something that covers, cushions or supports another device,” Sanchez said. “We’re asking what happens when the textile becomes the device itself with sensing, movement and mechanical function built directly into its structure.”

Today’s soft robotic systems often combine fabrics with separate sensors, actuators, electronics and structural components. That can make devices bulky and complicated to manufacture and can limit their ability to comfortably conform to different bodies. Sanchez’s team is taking a different approach. By carefully controlling yarn selection, stitch patterns and three-dimensional knit architecture, she aims to encode mechanical behavior into a textile as it is manufactured. Functional fibers, pneumatic channels and sensors could be integrated into the same knitted structure, allowing a fabric to bend, twist, contract or inflate while also sensing its own movement and interaction with a user.

This approach builds on years of Sanchez’s work in the field of textiles, materials science and robotics — and the unconventional path she took to get here.

Sanchez began using a sewing machine as a young child, and she initially studied fashion design as an undergraduate.

“I began college studying fashion at FIT before transferring to Cornell to study fiber science,” Sanchez said. “That shift helped me realize I could bring together my interests in design and engineering.”

She later earned graduate degrees at Harvard University, where she worked on soft robotic systems designed to assist human movement, before conducting postdoctoral research at Stanford University. Today, she directs Rice’s texlab, where she designs robotic textiles and soft wearable systems.

That combination of textile design and engineering shapes the new Toyota-supported project.

“Textiles are already extraordinarily good at interacting with the human body,” Sanchez said. “They stretch, conform, distribute forces and move with us. If we can add robotic functionality without losing those qualities, we can begin designing systems that are much more natural and comfortable for people to use.”

The 12-month project will focus first on integrating sensing and actuation — the ability to detect changes and produce movement — within the same 3D-knitted structures.

Using materials including conductive fibers, pneumatic channels and composite knitted architectures, Sanchez’s team plans to create textile modules capable of programmed sequences of motion, such as contracting, bending, twisting and inflating.

At the same time, embedded sensing could allow those structures to detect information such as strain, pressure, deformation and loading. Eventually, that capability could enable a robotic textile to sense what is happening to it and adjust its behavior in response.

Sanchez’s lab has already developed technologies featuring textile-based sensors, programmed textile actuators, morphing fabrics and knitted pneumatic actuators capable of producing specific motions based on their structure. At Rice, her group is also investigating AI-guided textile design and new manufacturing techniques for knitted robotic systems.

The fellowship will allow her to begin bringing those capabilities together into more integrated systems.

The second phase of the project will translate those textile systems into prototype technologies relevant to mobility. Possible applications include wearable devices that provide localized assistance to help a person move, seating or interior surfaces that change shape or stiffness in response to a user and soft safety structures that deploy or deform to absorb energy.

The prototypes will be developed in collaboration with Toyota researchers and evaluated for performance, sensing, manufacturability, weight, adaptability and safe interaction with people.

The research reflects a general shift toward designing robots that can operate more naturally alongside humans. For Sanchez, the project is part of a larger effort to expand what textiles can do.

“I’m continuously trying to understand the relationship between fibers and yarns and their structures so well that I can be really innovative and build something brand new,” she said. “Ultimately, I want to use textiles to create new kinds of machines and systems that can support people.”

For more information: Texlab

Image: Vanessa Sanchez in her lab at Rice.

Matergenics deploys first-of-its-kind in-steel hydrogen embrittlement sensor at italian green-hydrogen blending facility

Matergenics has deployed its hydrogen-in-steel monitoring sensor at a hydrogen-natural gas blending facility in Italy, marking the first operational use of the technology. Engineered by Techfem S.p.A., the facility blends green hydrogen into a natural gas network and is supported by continuous remote monitoring from Matergenics’ Hydrogen Solutions Division in Pittsburgh. The system uses continuous dilation measurements and HEILD-based analysis to help assess hydrogen embrittlement risks in operating steel piping.

Hydrogen blending is widely regarded as a near-term pathway for reducing the carbon intensity of existing natural gas infrastructure. However, introducing hydrogen into steel piping can increase susceptibility to hydrogen embrittlement—a degradation process in which absorbed hydrogen reduces ductility and fracture resistance and may contribute to crack initiation or accelerated crack growth without readily visible warning signs.

Conventional operating measurements, including pressure, flow, temperature, and leak detection, do not directly characterize hydrogen uptake or the evolving mechanical response of the steel. Matergenics’ monitoring technology is designed to help address this gap.

The sensor is bonded directly to the exterior of the pipe and continuously measures extremely small dimensional and strain changes associated with hydrogen interaction with the steel. The resulting data are securely transmitted to Matergenics’ Pittsburgh monitoring center, where they are evaluated using proprietary analytical methods based on HEILD—the Hydrogen-Enhanced Instability by Local Dilation framework.

HEILD relates localized, hydrogen-associated dilation and mechanical instability to the susceptibility of a specific material and component to hydrogen-assisted damage. Rather than relying solely on hydrogen pressure, exposure time, or other generalized operating parameters, the system evaluates the response of the actual steel component while it remains in service.

“For decades, the hydrogen-embrittlement community has largely had to infer risk from environmental conditions, laboratory testing, and indirect measurements,” said Dr. Michael McGuire, Chief Scientist at Matergenics. “This deployment gives us the ability to monitor the mechanical response of an operating steel pipe continuously and translate that response into actionable information for integrity management.”

The project combines Techfem’s expertise in hydrogen and hydrogen–natural gas infrastructure with Matergenics’ sensing, materials-testing, and analytical capabilities. Together, the technologies provide the facility operator with visibility into a degradation mechanism that conventional pressure, flow, and leak-monitoring systems are not designed to detect.

“This installation represents an important step toward condition-based integrity management for hydrogen infrastructure,” said Dr. Mehrooz Zamanzadeh, Founder and President of Matergenics. “Our objective is to help operators identify changes in hydrogen-related risk before they develop into cracking, leakage, or loss of containment.”

The installation builds on an ongoing hydrogen-monitoring collaboration between Matergenics and Techfem and supports Matergenics’ continuing development and validation of HEILD as a framework for evaluating hydrogen-assisted damage in ferritic, martensitic, and austenitic steels.

Matergenics and Techfem intend to evaluate the system’s in-service performance and explore its application to additional hydrogen-blending facilities, pipelines, storage systems, and other hydrogen-exposed assets.

ABOUT MATERGENICS, INC.

Matergenics, Inc. is a materials, corrosion, and failure-analysis engineering firm headquartered in Pittsburgh, Pennsylvania. Led by Dr. Mehrooz Zamanzadeh, FAMPP and FASM, the company provides corrosion assessment, materials testing, failure analysis, structural-integrity evaluation, and remote monitoring services. Matergenics’ Hydrogen Solutions Division focuses on hydrogen embrittlement research, accelerated testing, materials qualification, and in-service structural monitoring. Its technologies include HEILD—the Hydrogen-Enhanced Instability by Local Dilation framework—and the Circumferentially Pre-Cracked Round Bar methodology for accelerated determination of threshold stress-intensity behavior, K₁ₕ, in hydrogen environments.

ABOUT TECHFEM S.p.A.

Techfem S.p.A. is an Italian engineering company with more than 40 years of experience in strategic energy infrastructure. The company delivers engineering and project management services across the hydrogen, natural gas, CO₂, and power transmission sectors, supporting the development of secure and sustainable energy systems. With over 60 hydrogen projects in its portfolio, Techfem is active throughout the hydrogen value chain, from production and blending to transport and storage, while advancing innovative solutions through participation in national and European research and development programs.

For more information: Matergenics, Inc.

 

MIT researchers use AI to uncover atomic defects in materials

Researchers at the Massachusetts Institute of Technology built an AI model trained on 2,000 different semiconductor materials using data from a noninvasive neutron-scattering technique that can detect and classify up to six kinds of point defects in a material simultaneously, something that would be impossible using conventional techniques alone.

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Beyond silicon: Modeling the materials behind the future of electronics

As technology advances beyond traditional silicon-based electronics, organic semiconductors are emerging as a key material for innovations such as wearable sensors, implantable devices and foldable screens. Toulik Maitra, a Ph.D. student in chemical engineering at the University of California, Davis, is helping advance this field through computational modeling that explores how these materials behave at the molecular level. His research recently expanded through a collaboration with Germany’s Max Planck Institute, a world-renowned leader in polymer and organic electronics research, bringing the future of flexible and next-generation electronics one step closer to reality.

Silicon is an excellent semiconductor, capable of switching between conducting and blocking electricity. However, silicon atoms are locked together by covalent bonds, making them strong but also rigid. 

Organic semiconductors, on the other hand, are carbon-based materials that can perform the same electronic functions as silicon but are more flexible because their molecules are held together by weak attractions called van der Waals forces. 

“It’s the same force that lets a gecko stick to a smooth wall without any glue,” Maitra says. 

That flexibility also makes the materials much more difficult to model accurately.

“Due to van der Waals forces, at room temperature, the molecules vibrate, causing each electron cloud to shift in response to its neighbors, or polarization,” Maitra said. “It has a large effect on how charges move through the material and interact with light.” 

Capturing this behavior accurately in computer simulations is difficult, slowing the design of new organic semiconductor materials. Maitra’s goal is to computationally model the molecular behavior to design better materials before anyone steps into a lab. 

During a six-month appointment as a visiting fellow at the Max Planck Institute for Polymer Research in Mainz, Germany, Maitra and his collaborators set out to capture how shifts in polarization affect charge transport and light interactions. 

The international team developed a new computational framework that predicts how individual atoms respond to their molecular surroundings, enabling simulations to more accurately reflect the behavior of organic semiconductors in the real world.

The framework accounts for the unique environment surrounding each atom. It has proven more accurate than conventional methods, which assign the same electronic properties to broad categories of atoms. 

It also accurately models molecules in their neutral, charged and excited states — the same conditions they experience inside a working electronic device. When combined with machine learning, the framework can quickly predict these properties for new molecules, enabling researchers to identify promising materials before synthesizing them in the laboratory.

Maitra is already applying these improved modeling techniques to his doctoral research in the laboratory of Adam Moulé, professor of chemical engineering at UC Davis. There, he studies organic semiconductor materials for organic light-emitting diodes, or OLEDs, with a particular focus on thermally activated delayed fluorescence, or TADF, emitters and high-mobility molecules.

Currently, the highest-efficiency OLED displays often rely on rare metals such as iridium and platinum to produce bright, energy-efficient light. TADF materials offer a promising alternative, achieving similar performance with entirely organic molecules. 

By more accurately predicting how those molecules will behave before they are synthesized, Maitra hopes to help researchers accelerate the search for efficient OLED materials that reduce dependence on expensive, rare-earth materials.

“I am always excited to move the field forward,” Maitra said. “If this method works, then the next thing you want to model — device performance or vibration analysis — can be done in a better way.”

Maitra will be able to continue his collaboration with the Max Planck Institute at UC Davis in the Moulé Lab thanks to a UC Davis Dissertation Fellowship, which is awarded by UC Davis Graduate Studies to support a Ph.D. student for a year toward the end of their academic career.  

The fellowship gives Maitra the time to focus on publishing his research, completing his dissertation and preparing for a career advancing organic semiconductor technologies.

“I believe in this field,” Maitra said. “Working with organic semiconductors will make a better future.”

New method scales up twist-engineered oxide materials for future electronics

Researchers have expanded the field of twistronics by developing a method to manufacture oxide twistronic materials at much larger scales while precisely controlling the twist angles between layered materials. Twistronics focuses on how the alignment of two-dimensional materials influences their structural and electronic properties, and this new technique could help advance research and practical applications by making these materials easier to produce and study.

From weak forces to oxides

“The field of twistronics was developed using 2D materials that are bonded by weak van der Waals forces,” says Ruijuan Xu, corresponding author of a paper on the work and an assistant professor of materials science and engineering at North Carolina State University. “Our work here demonstrates it is possible to use layers of oxide materials that are connected by strong chemical bonds—while precisely controlling the twist angle between crystalline oxide membranes.

“The strong interlayer bonding we found between oxide layers suggests there may be entirely new interfacial phenomena to explore,” adds Xu. “We’ve demonstrated the ability to control many of the materials’ characteristics—including phase structure and domain configuration—in ways that offer new routes for designing materials and devices tailored to specific applications.”

Building large-area twisted membranes

For this work, the researchers synthesized crystalline sodium niobate (NaNbO3) membranes and used photolithography to create a set of visual markers along the perimeter of each membrane. One NaNbO3 membrane was then lifted and placed on top of another NaNbO3 membrane. The researchers monitored the alignment of the visual markers during assembly to precisely control the relative twist angle between the two layers. Once they established the desired angle, they performed a material-specific annealing process to establish strong chemical bonding between the layers.

“Scale matters for devices,” says Xu. “Because these crystalline membranes can be fabricated over large areas and transferred onto different supports, this approach provides a practical path toward twist-engineered oxide electronics.”

Atomic distortions at the interface

The researchers also used synchrotron X-ray diffraction techniques to capture what is happening at the interface between the two layers.

“We found that the bonds between the two layers are so strong that they are distorting the atomic structure of the material—creating a gradual rotation of the atomic lattice at the interface between the layers,” says Xu. “We also found changes to the phase structure of the material. It remains to be seen how this will affect material properties, but that’s something we are exploring.”

Extending the method beyond sodium niobate

The researchers note that while this work was done using NaNbO3 as a model, the technique could be extended to other complex oxides.

“Our work demonstrates a technique for creating large-area oxide twistronic materials with controlled twist angles and a strong chemical bond between layers,” says Xu. “It’s an exciting time for oxide twistronics, with new opportunities to engineer complex oxide functionalities through twist.”

For more information: ACS Nano

New state-of-the-art facility provides access to advanced materials, manufacturing tools

A new facility at Arizona State University’s Tempe campus will give researchers and corporate partners access to a wide range of advanced materials and manufacturing tools, supporting work with cutting-edge technologies. The Biodesign Institute marked the opening with a ribbon-cutting ceremony and facility tours earlier this month.

Managed by the Biodesign Center for Sustainable Macromolecular Materials and Manufacturing, or SM3, the facility houses tools that support research such as scanning electron microscopy, thermal analysis, light scattering, mechanical testing, gas permeability measurements, water uptake analysis and rheological testing to better understand and optimize material performance.

The lab also features cutting-edge additive manufacturing technologies, ranging from extrusion-based systems to light-driven 3D printers.

Among its most notable additions is the Cubicure Caligma printer, the first system of its kind in the United States capable of integrating extrusion and light-based printing at the micron scale, opening new possibilities for precision manufacturing and materials development.

The new laboratory represents the transformation of the former ASU Biodesign Clinical Testing Lab — best known as the site of the university’s large-scale COVID-19 saliva testing operations — into a state-of-the-art research hub dedicated to advancing sustainable materials innovation.

The facility is already serving a growing community of researchers, with approximately 60 faculty members, students and staff from across ASU utilizing the space and its resources.

By bringing together expertise in materials science, engineering, chemistry and manufacturing, the center aims to accelerate the development of sustainable products and technologies while strengthening Arizona’s innovation ecosystem.

During the ceremony, attendees heard from Biodesign leaders and industry partners about the importance of investing in shared research infrastructure that can support both fundamental discovery and commercial translation.

“We’re focused on sustainability,” said Tim Long, director of the Biodesign Center for Sustainable Macromolecular Materials and Manufacturing. “And these days what does that mean? That means resiliency. It means supply chain. It means using our resources more effectively. It means being more competitive as a nation, more competitive with our companies and more effectively educating our students, the future generation, the future workforce.”

The new laboratory is also expected to serve as a catalyst for expanded partnerships with leading instrument manufacturers and private industry, helping drive Arizona-based product innovation and workforce development.

Industry representatives participating in the event highlighted the value of collaborative research environments that connect academic expertise with real-world challenges.

“What this expansion does in practice is reduce friction,” said Jeff Addy, an ASU alumnus and research and development manager from Cargill Bioindustrial. “It means you can move from an idea to real data faster, ask better questions and iterate more quickly. That changes the kind of work you can do, not just how fast you can do it.”

Following the ribbon cutting, guests toured the laboratory and explored the technologies that will support the next generation of sustainable materials research and manufacturing at ASU.

For more information: Biodesign Center for Sustainable Macromolecular Materials and Manufacturing

Image: Industry collaborators tour the Biodesign Institute’s new shared manufacturing lab managed by the Center for Sustainable Macromolecular Materials and Manufacturing on Tuesday, June 9. The facility provides access to advanced tools that support electron microscopy, thermal analysis, light scattering, mechanical testing, gas permeability, water uptake, rheology and 3D printing. Photo by Charlie Leight/ASU News

Designing matter at the nanoscale

Toni Taylor, a Los Alamos National Laboratory fellow and physicist, recalls that early terahertz research was hindered by the lack of modulators—devices that control light’s amplitude, phase or frequency—making it difficult for this promising band to reliably carry information for communications and medical applications. Situated between microwaves and infrared light, the terahertz range is too fast for conventional electronics and too slow for traditional optics, leaving it largely unmastered compared with other parts of the electromagnetic spectrum that drove advances such as radar and photonics. Because terahertz waves pass through typical modulator materials with little absorption or reflection, scientists have had limited ability to control them, creating what is known as the “terahertz gap” and leaving significant technological potential untapped.

Terahertz waves oscillate trillions of times per second, hundreds of times faster than the microwave-frequency systems used in today’s wireless networks. In principle, that behavior means they could carry vastly more information than today’s fastest consumer networks. But communications is only part of the appeal. Like x-rays, terahertz radiation can penetrate many nonmetallic materials, but unlike x-rays, it doesn’t ionize atoms, meaning it doesn’t change the materials’ structure. In theory, that makes terahertz radiation well-suited to nondestructive probing of delicate materials, from biological tissue to concealed explosives. “There just weren’t good photonics devices there,” Taylor says. “At the time, neither naturally occurring materials nor manmade alloys interacted strongly enough in that band to control it.”

By the early 2000s, when Taylor and coworkers began working in the terahertz band, the computer revolution had pushed technology to an inflection point. Moore’s Law was still busy shrinking transistors, but devices had reached dimensions small enough that quantum effects shaped performance. Advances could no longer come from simply making components smaller. To keep accelerating computation, materials had to be designed down to the level of their very atoms.

For the first time, nanoscale engineering, working at dimensions of billionths of a meter, where materials behave in fundamentally new ways, was becoming practical. Long before nano products were built, scientists could model them on supercomputers that predicted how electrons and electromagnetic waves would behave in such tiny structures. Cleanroom fabrication techniques refined by the microelectronics industry were building structures smaller than one hundred nanometers with remarkable precision, while scanning tunneling microscopes and atomic force microscopes made it possible not only to image the placements of individual atoms but, in some cases, to nudge them deliberately into place.

All of these technological factors, plus the promise of the capabilities they enabled, led the Department of Energy’s Office of Science to create the Center for Integrated Nanotechnologies, a centerpiece facility among a national network of nanoscale research centers. Opened in 2004 and jointly operated by Los Alamos and Sandia national laboratories, CINT was built as a user facility, a place where scientists from around the world could propose ideas and gain access to specialized tools and expertise. Housed within this tightly integrated environment, researchers could move from theory to synthesis to fabrication to characterization—all at the nanoscale.

For researchers like Taylor, CINT turned the terahertz gap from an abstract limitation into an engineering problem. “All of the tools needed to develop the modulators were at CINT,” Taylor says. Her team’s work on the project began in earnest in 2006, when a postdoctoral researcher named Willie Padilla arrived at Los Alamos with expertise in metamaterials: artificially structured surfaces engineered to manipulate electromagnetic waves in ways natural materials cannot.

The way a material traditionally absorbs or reflects light is dictated by its atomic composition—the electronic transitions and vibrational modes built into its chemistry.  Padilla’s insight was that they no longer had to rely on the electronic structure of naturally occurring materials to support a resonance at terahertz frequencies. They could engineer a material instead.

Using CINT’s modeling tools, he and his collaborators designed metallic patterns sized to resonate at terahertz frequencies: tiny, repeating loops and gaps etched into a thin film of gold. When a terahertz wave struck the patterned surface, its oscillating electric field drove the metal’s free electrons back and forth. If the geometry was right—if the loops and gaps were sized precisely for that frequency—the electrons would move in sync with the incoming wave. The energy in the terahertz waves that would otherwise have passed quietly through the material was briefly captured, scattered, or absorbed. Like radio antennas tuned to a single station, the gold resonators responded strongly only at the frequency dictated by their shape.

But this was still a passive response, like a filter or detector. The resonator device could isolate or suppress an individual frequency, but couldn’t change that frequency in real time. Without time-dependent control, it wasn’t yet useful for information transmission. To do that, Padilla, along with his coworkers Hou-Tong Chen, Richard Averitt, and Taylor had to find a way to modulate the signal itself.

The solution lay in setting the patterned metal resonator atop a semiconductor substrate. By injecting charge into that substrate—electrically or with an ultrafast optical pulse—the team temporarily increased its conductivity. That shift altered how freely the electrons in the resonators could oscillate. When the substrate became more conductive, the oscillations dissipated energy more quickly and the response weakened; when it was less conductive, the resonance sharpened. In practical terms, a static surface had become a controllable gate. A region of the spectrum long considered technologically awkward could now be modulated in real time. The work culminated in a 2006 paper demonstrating active control of terahertz radiation.

What followed was not just a device, but a new way of thinking about matter: that it could be modified at the nanoscale to realize ideas once confined to theory. Taylor’s group went on to pursue higher-speed modulators, tunable filters, polarization rotators, and broadband converters. They extended the same nanoscale design principles to problems across national security and optical communications. More recently, collaborators demonstrated structures that can generate and steer terahertz radiation with unprecedented control. That approach has contributed to advances in security imaging seen at airports, materials diagnostics, and next-generation wireless research. Recent experimental terahertz systems achieved data rates exceeding 100 gigabits per second, far beyond typical consumer wireless speeds.

Terahertz modulation is only one expression of CINT’s broader vision. Across the Center, researchers have applied the same integration of modeling, fabrication, and measurement to problems ranging from quantum dots to structural materials. Victor Klimov and Jennifer Hollingsworth engineered quantum dots whose optical gain and emission can be tuned with atomic precision, advancing solar technologies, microelectronics, and quantum information science. Other Los Alamos teams designed nanoscale defect architectures to strengthen materials and built atom-scale emitters matched to fiber-optic telecommunications bands. Each effort differs in application, but they share a methodology enabled by CINT: design at the nanoscale, fabricate precisely, measure rigorously, iterate quickly.

“We wanted to understand the materials and then design them to do the thing that we wanted them to do,” Taylor says. The science has advanced since the early days of terahertz modulators. The ambition remains the same: to design matter itself.

For more information: Los Alamos National Laboratory 

Nikhil Bajaj’s $649K NSF CAREER Award reverses the design process for devices from microsensors to aircraft wings

Nikhil Bajaj, an assistant professor of mechanical engineering and materials science at the University of Pittsburgh’s Swanson School of Engineering, studies nonlinear systems that shift behavior once a threshold is crossed—phenomena seen across disciplines in devices that rely on bifurcation to enhance sensitivity and performance. He has received a $649,684 National Science Foundation CAREER Award to rethink how these systems are designed, moving away from trial-and-error tuning toward an approach that starts with a desired behavior and engineers backward. His framework targets applications such as micro-electro-mechanical systems, including ultrasensitive gas leak detectors capable of identifying hazardous compounds at parts-per-billion levels, as well as energy harvesters and aerospace structures.

In a system with bifurcations, a quantitative change produces a qualitative one: a change in the value of the input changes the type of outcome. Once a certain threshold is met, the system doesn’t do more of what it was doing; it instead does something different. For example, a somewhat flexible column loaded with heavier and heavier weights will compress more and more, but once a specific load is placed on it, it will move in a different way, bulging out to one side or buckling.

Today, researchers can characterize these kinds of systems using a lot of trial and error and analogies to previous systems. “Say I’m building a car, and I want it to have 400 horsepower,” Bajaj said. If he didn’t know how to hit that number, he might take any engine and keep tweaking it, tightening something here, disconnecting a part there, until it worked. And horsepower is an easy case, a smooth dial you can turn up or down. The challenge multiplies when the goal is a threshold behavior: getting a system to switch into a new kind of motion at exactly the right input, and not a moment before.

“Designing in bifurcation behavior can feel a bit like working in the dark,” Bajaj said. Even so, the field has made remarkable progress. Across nonlinear systems, libraries of relationships have accumulated for many decades as researchers test inputs and observe outputs via theory and experiment. They’ve found that systems with bifurcations of all kinds (a wing vibrating erratically at speed, a material buckling under pressure, a neuron firing in the brain) seem to be governed by similar principles. The equations aren’t identical, but when systems engineers compare notes, they find meaningful similarities behind the different variables and outputs.

“We play the same mathematical games, just on different fields,” Bajaj said. At a nonlinear dynamics conference, he might have a specific engineering question on his mind. “But then I could run into someone doing the same thing on a biological system and I think, ‘I can use their method to apply to my problem.’”

The award also supports an education plan that spans the length of the pipeline. Bajaj will carry the science of nonlinear behavior (the buckling and the sudden shifts that turn up everywhere from bridges to neurons) to K–12 students and the public through science center and library exhibits, and will fold the same design methods into undergraduate and graduate coursework. A layered mentorship model reaching students at different stages aims to broaden participation in STEM, giving newcomers both a way in and a reason to stay.

Bajaj will use his CAREER Award to develop a unified computational framework for designing nonlinear systems from a desired behavior, rather than discovering their behavior through trial and error. “I want to pick all my parameters, all the knobs I can turn, so that it does the things I want it to do and not necessarily the things that are undesirable.” The framework is intentionally general; he will demonstrate the approaches on small and large scales, from MEMS gas sensors at the micrometer scale to flutter in aircraft wings.

For more information: U.S. National Science Foundation

Team builds best-performing detection system for next-generation accelerators

Physicists at UC Santa Cruz and partner institutions in California and New Mexico have developed a new detection system designed to improve next-generation particle accelerators, enabling more precise studies of fundamental biological and chemical processes and supporting advances in materials science and energy research. The effort, led by the Advanced Accelerator Diagnostics Collaboration, which includes two University of California campuses and three U.S. national laboratories, addresses the growing need for high-rate beam diagnostics as accelerator performance increases from 120 pulses per second to as many as 1 million pulses per second, a jump that strains existing diagnostic systems.

“It really highlights the power of collaboration between universities and national laboratories,” said Bruce Schumm, the Long Family Professor of Experimental Physics. “If you took away Lawrence Berkeley Lab, if you took away Los Alamos, if you took away UC Davis, any of those, the whole thing would have fallen apart.”

The fruits of this years-long collaboration are nothing less than the best-performing high-bandwidth particle detection system built to date. The system combines artificial diamonds, custom microchips, and cutting-edge assembly techniques into a compact detector designed for measuring the properties of the beams shot by advanced accelerators like the Linac Coherent Light Source II at SLAC National Accelerator Laboratory in Menlo Park.

Need for speed

As next-generation particle accelerators continue to develop, they will have faster and faster bursts of charged particles that are close to each other in time. This means the researchers using them will need to create new, faster ways to measure these beams and control their properties.

“Nobody was building things that can measure, diagnose the beams and help control the accelerator, and also help the experimenters to unravel the data,” said Schumm.

At these high rates of beam repetition—eventually reaching beyond one billion times per second—existing detection systems fail. To overcome that barrier, the Advanced Accelerator Diagnostics Collaboration set out to redesign the entire detection chain from the sensor material itself, to the electronics used to read out the signal.

“It required developing a new approach to processing the signal, and also a new integrated circuit chip that we designed ourselves and then characterized,” said Schumm. “This is the first time we put it all together and put it into a beam.”

For more information: Physical Review Accelerators and Beams

Image: The detection system along with associated hardware for electronic conditioning and control. Photo by Carolyn Lagattuta.